Articles | Volume 14, issue 6
https://doi.org/10.5194/bg-14-1365-2017
© Author(s) 2017. This work is distributed under
the Creative Commons Attribution 3.0 License.
the Creative Commons Attribution 3.0 License.
https://doi.org/10.5194/bg-14-1365-2017
© Author(s) 2017. This work is distributed under
the Creative Commons Attribution 3.0 License.
the Creative Commons Attribution 3.0 License.
Research article
| 
20 Mar 2017
Research article |
| 20 Mar 2017
Gas chromatography vs. quantum cascade laser-based N2O flux measurements using a novel chamber design
Christian Brümmer
CORRESPONDING AUTHOR
Thünen Institute of Climate-Smart Agriculture, Braunschweig,
Germany
Bjarne Lyshede
Thünen Institute of Climate-Smart Agriculture, Braunschweig,
Germany
Dirk Lempio
Thünen Institute of Climate-Smart Agriculture, Braunschweig,
Germany
Jean-Pierre Delorme
Thünen Institute of Climate-Smart Agriculture, Braunschweig,
Germany
Jeremy J. Rüffer
Thünen Institute of Climate-Smart Agriculture, Braunschweig,
Germany
previously published under the name Jeremy Smith
Roland Fuß
Thünen Institute of Climate-Smart Agriculture, Braunschweig,
Germany
Antje M. Moffat
Thünen Institute of Climate-Smart Agriculture, Braunschweig,
Germany
Miriam Hurkuck
Thünen Institute of Climate-Smart Agriculture, Braunschweig,
Germany
Andreas Ibrom
Department of Environmental Engineering, Technical University of
Denmark, Lyngby, Denmark
Per Ambus
Department of Geosciences and Natural Resource Management, University
of Copenhagen, Copenhagen, Denmark
Heinz Flessa
Thünen Institute of Climate-Smart Agriculture, Braunschweig,
Germany
Werner L. Kutsch
Thünen Institute of Climate-Smart Agriculture, Braunschweig,
Germany
Integrated Carbon Observation System, ICOS ERIC Head office, Helsinki,
Finland
Viewed
Total article views: 4,447 (including HTML, PDF, and XML)
Cumulative views and downloads
(calculated since 06 Jul 2016)
| HTML | XML | Total | Supplement | BibTeX | EndNote | |
|---|---|---|---|---|---|---|
| 2,468 | 1,779 | 200 | 4,447 | 445 | 118 | 141 |
- HTML: 2,468
- PDF: 1,779
- XML: 200
- Total: 4,447
- Supplement: 445
- BibTeX: 118
- EndNote: 141
Total article views: 3,190 (including HTML, PDF, and XML)
Cumulative views and downloads
(calculated since 20 Mar 2017)
| HTML | XML | Total | Supplement | BibTeX | EndNote | |
|---|---|---|---|---|---|---|
| 2,095 | 904 | 191 | 3,190 | 445 | 116 | 134 |
- HTML: 2,095
- PDF: 904
- XML: 191
- Total: 3,190
- Supplement: 445
- BibTeX: 116
- EndNote: 134
Total article views: 1,257 (including HTML, PDF, and XML)
Cumulative views and downloads
(calculated since 06 Jul 2016)
| HTML | XML | Total | BibTeX | EndNote | |
|---|---|---|---|---|---|
| 373 | 875 | 9 | 1,257 | 2 | 7 |
- HTML: 373
- PDF: 875
- XML: 9
- Total: 1,257
- BibTeX: 2
- EndNote: 7
Cited
17 citations as recorded by crossref.
- Global Research Alliance N2O chamber methodology guidelines: Recommendations for air sample collection, storage, and analysis M. Harvey et al. 10.1002/jeq2.20129
- Reconciling annual nitrous oxide emissions of an intensively grazed dairy pasture determined by eddy covariance and emission factors A. Wecking et al. 10.1016/j.agee.2019.106646
- Diurnal variability in soil nitrous oxide emissions is a widespread phenomenon Y. Wu et al. 10.1111/gcb.15791
- A Portable Laser Spectroscopic System for Measuring Nitrous Oxide Emissions on Fertilized Cropland G. Stiefvater et al. 10.3390/s23156686
- A novel injection technique: using a field-based quantum cascade laser for the analysis of gas samples derived from static chambers A. Wecking et al. 10.5194/amt-13-5763-2020
- Development of a Laser Gas Analyzer for Fast CO2 and H2O Flux Measurements Utilizing Derivative Absorption Spectroscopy at a 100 Hz Data Rate M. Li et al. 10.3390/s21103392
- Efficacy of agronomic strategies for mitigation of after-harvest N 2 O emissions of winter oilseed rape B. Vinzent et al. 10.1016/j.eja.2017.06.009
- Global Research Alliance N2O chamber methodology guidelines: Considerations for automated flux measurement P. Grace et al. 10.1002/jeq2.20124
- Are there memory effects on greenhouse gas emissions (CO<sub>2</sub>, N<sub>2</sub>O and CH<sub>4</sub>) following grassland restoration? L. Merbold et al. 10.5194/bg-18-1481-2021
- Soil N2O emissions in Mediterranean arable crops as affected by reduced tillage and N rate I. Volpi et al. 10.1007/s10705-019-10032-1
- Introduction of a guideline for measurements of greenhouse gas fluxes from soils using non‐steady‐state chambers M. Maier et al. 10.1002/jpln.202200199
- Effects of clear-fell harvesting on soil CO<sub>2</sub>, CH<sub>4</sub>, and N<sub>2</sub>O fluxes in an upland Sitka spruce stand in England S. Yamulki et al. 10.5194/bg-18-4227-2021
- Analysis of uncertainty for N2O fluxes measured with the closed‐chamber method under field conditions: Calculation method, detection limit, and spatial variability. C. Lammirato et al. 10.1002/jpln.201600499
- A new methodology for organic soils in national greenhouse gas inventories: Data synthesis, derivation and application B. Tiemeyer et al. 10.1016/j.ecolind.2019.105838
- Forest-floor respiration, N2O fluxes, and CH4 fluxes in a subalpine spruce forest: drivers and annual budgets L. Krebs et al. 10.5194/bg-21-2005-2024
- Improved parameterization of the commonly used exponential equation for calculating soil-atmosphere exchange fluxes from closed-chamber measurements A. Moffat & C. Brümmer 10.1016/j.agrformet.2017.03.005
- Can nitrogen input mapping from aerial imagery improve nitrous oxide emissions estimates from grazed grassland? J. Maire et al. 10.1007/s11119-022-09908-0
17 citations as recorded by crossref.
- Global Research Alliance N2O chamber methodology guidelines: Recommendations for air sample collection, storage, and analysis M. Harvey et al. 10.1002/jeq2.20129
- Reconciling annual nitrous oxide emissions of an intensively grazed dairy pasture determined by eddy covariance and emission factors A. Wecking et al. 10.1016/j.agee.2019.106646
- Diurnal variability in soil nitrous oxide emissions is a widespread phenomenon Y. Wu et al. 10.1111/gcb.15791
- A Portable Laser Spectroscopic System for Measuring Nitrous Oxide Emissions on Fertilized Cropland G. Stiefvater et al. 10.3390/s23156686
- A novel injection technique: using a field-based quantum cascade laser for the analysis of gas samples derived from static chambers A. Wecking et al. 10.5194/amt-13-5763-2020
- Development of a Laser Gas Analyzer for Fast CO2 and H2O Flux Measurements Utilizing Derivative Absorption Spectroscopy at a 100 Hz Data Rate M. Li et al. 10.3390/s21103392
- Efficacy of agronomic strategies for mitigation of after-harvest N 2 O emissions of winter oilseed rape B. Vinzent et al. 10.1016/j.eja.2017.06.009
- Global Research Alliance N2O chamber methodology guidelines: Considerations for automated flux measurement P. Grace et al. 10.1002/jeq2.20124
- Are there memory effects on greenhouse gas emissions (CO<sub>2</sub>, N<sub>2</sub>O and CH<sub>4</sub>) following grassland restoration? L. Merbold et al. 10.5194/bg-18-1481-2021
- Soil N2O emissions in Mediterranean arable crops as affected by reduced tillage and N rate I. Volpi et al. 10.1007/s10705-019-10032-1
- Introduction of a guideline for measurements of greenhouse gas fluxes from soils using non‐steady‐state chambers M. Maier et al. 10.1002/jpln.202200199
- Effects of clear-fell harvesting on soil CO<sub>2</sub>, CH<sub>4</sub>, and N<sub>2</sub>O fluxes in an upland Sitka spruce stand in England S. Yamulki et al. 10.5194/bg-18-4227-2021
- Analysis of uncertainty for N2O fluxes measured with the closed‐chamber method under field conditions: Calculation method, detection limit, and spatial variability. C. Lammirato et al. 10.1002/jpln.201600499
- A new methodology for organic soils in national greenhouse gas inventories: Data synthesis, derivation and application B. Tiemeyer et al. 10.1016/j.ecolind.2019.105838
- Forest-floor respiration, N2O fluxes, and CH4 fluxes in a subalpine spruce forest: drivers and annual budgets L. Krebs et al. 10.5194/bg-21-2005-2024
- Improved parameterization of the commonly used exponential equation for calculating soil-atmosphere exchange fluxes from closed-chamber measurements A. Moffat & C. Brümmer 10.1016/j.agrformet.2017.03.005
- Can nitrogen input mapping from aerial imagery improve nitrous oxide emissions estimates from grazed grassland? J. Maire et al. 10.1007/s11119-022-09908-0
Latest update: 20 Nov 2024
Short summary
We present a novel chamber design for measuring soil–atmosphere N2O fluxes and compare the performance of a commonly applied gas chromatography (GC) setup with laser-based (QCL) concentration detection. While GC was still a useful method for longer-term investigations, we found that closure times of 10 min and sampling every 5 s is sufficient when using a QCL system. Further, extremely low standard errors (< 2 % of flux value) were observed regardless of linear or exponential flux calculation.
We present a novel chamber design for measuring soil–atmosphere N2O fluxes and compare the...
Altmetrics
Final-revised paper
Preprint